Fundamentals of Fourier transform infrared spectroscopy [electronic resource] / Brian C. Smith.

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Edición:2nd ed.
Publicado: Boca Raton, FL : CRC Press, c2011.
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Formato: Electrónico eBook

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100 1 |a Smith, Brian C. 
245 1 0 |a Fundamentals of Fourier transform infrared spectroscopy  |h [electronic resource] /  |c Brian C. Smith. 
250 |a 2nd ed. 
260 |a Boca Raton, FL :  |b CRC Press,  |c c2011. 
300 |a 1 online resource (xiii, 182 p.) :  |b ill. 
504 |a Includes bibliographical references and index. 
505 0 0 |g Machine generated contents note:  |g ch. 1  |t Introduction to Infrared Spectroscopy --  |g I.  |t Terms and Definitions --  |g II.  |t The Properties of Light --  |g III.  |t What Is an Infrared Spectrum? --  |g IV.  |t What Are Infrared Spectra Used For? --  |g V.  |t The Advantages and Disadvantages of Infrared Spectroscopy --  |g VI.  |t The Advantages and Disadvantages of FTIR --  |g A.  |t The Advantages of FTIRs --  |g B.  |t The Disadvantage of FTIR --  |g VII.  |t FTIR: The Rest of the Story --  |t References --  |g ch. 2  |t How an FTIR Works --  |g I.  |t Interferometers and Interferograms --  |g A.  |t How Many Scans Should Be Used? --  |g II.  |t How an Interferogram Becomes a Spectrum --  |g A.  |t Scanning Advice --  |g III.  |t Instrumental Resolution --  |g A.  |t What Determines Resolution in an FTIR Scan? --  |g B.  |t What Resolution Should Be Used? --  |g IV.  |t FTIR Trading Rules --  |g V.  |t FTIR Hardware --  |g A.  |t Interferometers --  |g B.  |t Infrared Sources --  |g C.  |t Beamsplitters --  |g D.  |t Infrared Detectors --  |g E.  |t The Laser --  |g VI.  |t Testing Instrument Quality and Troubleshooting --  |t References --  |g ch. 3  |t Proper Use of Spectral Processing 
505 0 0 |g I.  |t The Rules of Spectral Processing --  |g II.  |t Spectral Subtraction --  |g A.  |t Subtraction Artifacts --  |g III.  |t Baseline Correction --  |g IV.  |t Smoothing --  |g V.  |t Spectral Derivatives --  |g VI.  |t Deconvolution --  |g A.  |t Guidance, Precautions, and Limitations --  |g VII.  |t Spectral Library Searching --  |g A.  |t The Search Process --  |g B.  |t Interpreting Library Search Results --  |g VIII.  |t Analysis of Mixtures: Subtract and Search Again --  |t References --  |g ch. 4  |t Preparing Samples Properly --  |g I.  |t Transmission Sampling Overview --  |g A.  |t Windows, Cells, and Materials for Transmission Analysis --  |g II.  |t Transmission Analysis of Solids and Powders --  |g A.  |t KBr Pellets --  |g 1.  |t Mechanical Grinding --  |g 2.  |t Advantages and Disadvantages of KBr Pellets --  |g B.  |t Mulls --  |g 1.  |t The Split Mull Method --  |g III.  |t Transmission Analysis of Polymers --  |g A.  |t The Cast Film Method --  |g B.  |t The Heat and Pressure Method --  |g IV.  |t Transmission Analysis of Liquids --  |g A.  |t Capillary Thin Films --  |g B.  |t Sealed Liquid Cells --  |g V.  |t Transmission Analysis of Gases and Vapors --  |g VI.  |t Reflectance Analysis --  |g A.  |t Different Types of Reflectance --  |g B.  |t Advantages and Disadvantages of Reflectance Sampling 
505 0 0 |g VII.  |t Specular Reflectance --  |g VIII.  |t Diffuse Reflectance (DRIFTS) --  |g A.  |t Abrasive Sampling --  |g IX.  |t Attenuated Total Reflectance (ATR) --  |g A.  |t Depth of Penetration --  |g X.  |t Applications of ATR --  |g A.  |t Liquids --  |g B.  |t Semi-Solids --  |g C.  |t Polymers --  |g D.  |t Powders --  |g XI.  |t ATR: Advantages and Disadvantages --  |g XII.  |t FTIR Sample Preparation: Overview and Recommendations --  |t References --  |g ch. 5  |t Quantitative Infrared Spectroscopy --  |g I.  |t Terms and Definitions --  |g II.  |t Beer's Law --  |g III.  |t Calibration and Prediction with Beer's Law --  |g A.  |t Calibration --  |g B.  |t Prediction --  |g C.  |t An Experimental Protocol for Single Component Analyses --  |g 1.  |t Analyzing for a Single Analyte --  |g IV.  |t Measuring Absorbances Properly --  |g A.  |t Peak Areas versus Peak Heights --  |g B.  |t Dealing with Overlapped Peaks --  |g V.  |t Avoiding Experimental Errors --  |t References --  |g ch. 6  |t Infrared Microscopy --  |g I.  |t Hyphenated Infrared Techniques --  |g II.  |t Infrared Microscopy Instrumentation --  |g III.  |t Sample Preparation --  |g IV.  |t Applications --  |g V.  |t Infrared Mapping and Imaging --  |t References. 
520 |a Reflecting the myriad changes and advancements in the technologies involved in FTIR, particularly the development of diamond ATRs, this second edition of Fundamentals of Fourier Transform Infrared Spectroscopy has been extensively rewritten and expanded to include new topics and figures as well as updates of existing chapters. Designed for those new to FTIR, but with enough reference material to appeal to journeyman and expert spectroscopists, this book does not demand any extensive familiarity with chemistry or physics. Specializing in concise and comprehensible explanations of FTIR topics, tthe author introduces the field of infrared spectroscopy, including the strengths and weaknesses of FTIR as a chemical analysis technique. He then describes the instrument itself and explores topics such as how an interferometer generates a spectrum, optimization of spectral quality, and which tests are used to monitor instrument health.The book discusses how to properly use spectral processing to increase the information of a spectrum without damaging the data and takes considerable care in instructing on sample preparation, as good sample preparation constitutes half the battle in extracting good data. The final chapters examine single analyte quantitative analysis and conclude with an overview of infrared microscopy. 
650 0 |a Fourier transform infrared spectroscopy. 
776 0 8 |i Print version:  |a Smith, Brian C.  |t Fundamentals of Fourier transform infrared spectroscopy.  |d Boca Raton : CRC Press, c2011  |z 9781420069297  |w (DLC) 2010044423  |w (OCoLC)166358484 
856 4 0 |y Connect to electronic resource  |u http://www.canterbury.eblib.com.au/patron/FullRecord.aspx?p=681305  |t 0 
942 |a 30112011 
945 |b DO NOT SET  |c Manual 
991 |a 2011-11-30 
992 |a Created by nimo, 30/11/2011. Updated by nimo, 01/12/2011. 
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